SiCp/AZ91镁基复合材料的高温变形行为及组织演变
High Temperature Deformation and Microstructure Evolution of SiCp/AZ91 Magnesium Matrix Composites
- 2022年42卷第7期 页码:827-831
纸质出版日期: 2022
DOI: 10.15980/j.tzzz.2022.07.008
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纸质出版日期: 2022
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采用Gleeble-3800型热模拟试验机对搅拌铸造SiCp/AZ91镁基复合材料在250~400℃、应变速率为0.001~1 s-1下进行了单向压缩变形处理,观察了复合材料变形过程中的微观组织演变,揭示了SiCp/AZ91镁基复合材料的高温变形机制。结果表明,铸态SiCp/AZ91镁基复合材料中只有Mg相和SiC相;应变速率为0.001 s-1时,在压缩温度为250℃已经发生了部分再结晶,在350℃时发生完全再结晶,提高至400℃时,再结晶晶粒快速长大;压缩温度为250℃和350℃时,降低应变速率更加有利于SiCp/AZ91镁基复合材料的动态再结晶。其应力因子n为5,真激活能Q为91 kJ/mol,变形机制为晶界扩散控制的位错攀移。
The unidirectional compression deformation of SiCp/AZ91 magnesium matrix composites was carried out by Gleeble-3800 thermal simulation testing machine under the deformation temperature of 250 ℃~400 ℃ and the strain rate of 0.001 s-1~1 s-1. The microstructure evolution during the deformation process was observed and the high temperature deformation mechanism of SiCp/AZ91 magnesium matrix composites was revealed. The results indicate that there are only Mg phase and SiC phase in as-cast SiCp/AZ91 magnesium matrix composites. When the strain rate is 0.001 s-1, composites are partially recrystallized at 250 ℃, which are fully recrystallized at 350 ℃. When the compression temperature is increased to 400 ℃, the recrystallized grains grow rapidly. The reduction of strain rate is beneficial to dynamic recrystallization of SiCp/AZ91 magnesium matrix composites at 250 ℃ and 350 ℃, where the stress factor is 5, the true activation energy Q is 91 kJ/mol, and the deformation mechanism is dislocation climbing controlled by grain boundary diffusion.
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