Mg<sub>3</sub>Sb<sub>2</sub>增强镁基复合材料合成机制研究

池园园; 龙威; 周小平

doi:10.15980/j.tzzz.2018.10.017

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Mg₃Sb₂增强镁基复合材料合成机制研究
Synthesis Mechanism of Mg₃Sb₂ Reinforced Magnesium Matrix Composites
2018年38卷第10期页码：1105-1108
纸质出版日期： 2018 ，
DOI： 10.15980/j.tzzz.2018.10.017

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[1]池园园,龙威,周小平.Mg_3Sb_2增强镁基复合材料合成机制研究[J].特种铸造及有色合金,2018,38(10):1105-1108.

Chi Yuanyuan, Long Wei, Zhou Xiaoping. Synthesis Mechanism of Mg₃Sb₂ Reinforced Magnesium Matrix Composites[J]. Special Casting & Nonferrous Alloys, 2018,38(10):1105-1108.
[1]池园园,龙威,周小平.Mg_3Sb_2增强镁基复合材料合成机制研究[J].特种铸造及有色合金,2018,38(10):1105-1108. DOI： 10.15980/j.tzzz.2018.10.017.

Chi Yuanyuan, Long Wei, Zhou Xiaoping. Synthesis Mechanism of Mg₃Sb₂ Reinforced Magnesium Matrix Composites[J]. Special Casting & Nonferrous Alloys, 2018,38(10):1105-1108. DOI： 10.15980/j.tzzz.2018.10.017.

摘要

采用原位反应法制备不同Mg

体积分数的镁基复合材料。计算了不同温度下反应的吉布斯自由能和不同Sb含量的绝热温度

对复合材料进行X射线衍射（XRD）和差示扫描量热法（DSC）的检测。结果表明

原位反应方法可制备不同Mg

体积分数的镁基复合材料;Mg和Sb结合生成Mg

的反应能自发进行;Sb含量分别为7.7%、15.4%、23.1%时

Mg-Sb合成反应不能自蔓延发生

金属间化合物Mg

的合成温度分别为544.58、621.84和666.14℃。

Abstract

Magnesium matrix composites with different volume fractions of Mg

by in-situ method were prepared.The Gibbs free energy at different temperatures and adiabatic temperature of different Sb contents were calculated

and the composites were examined by X ray diffraction（XRD）and differential scanning calorimetry（DSC）.The results reveal that the magnesium matrix composites with different volume fractions of Mg

can be prepared by in-situ method.The 3Mg+2Sb=Mg

reaction can be carried out spontaneously.When the Sb content is 7.7%

15.4%and 23.1%

the synthesis reaction of Mg-Sb cann’t occur spontaneously.The synthesis temperature of intermetallic compound Mg

is544.58℃

621.84℃and 666.14℃

respectively.