Shao Qi, Yin Jian, Liu Fei. Effects of Ni Additions on the Microstructure of Mg-Er-Ni Alloys[J]. Special Casting & Nonferrous Alloys, 2018,38(6):684-687.
Shao Qi, Yin Jian, Liu Fei. Effects of Ni Additions on the Microstructure of Mg-Er-Ni Alloys[J]. Special Casting & Nonferrous Alloys, 2018,38(6):684-687. DOI: 10.15980/j.tzzz.2018.06.029.
Ni含量对Mg-Er-Ni合金组织的影响
摘要
采用光学显微镜(OM)、X射线衍射仪(XRD)、扫描电镜(SEM)和能谱分析(EDS)等手段
研究了Ni含量对Mg
98-x
Er
2
Ni
x
(摩尔分数
下同
x=0
0.25
0.5
1)合金组织的影响。结果表明
铸态Mg
98
Er
2
合金组织为初生树枝状α-Mg相
晶内出现成分偏析
Mg
97.75
Er
2
Ni
0.25
、Mg
97.5
Er
2
Ni
0.5
和Mg
97
Er
2
Ni
1
三种合金的组成相主要是α-Mg相和LPSO相
第二相的面积分数分别为12%、19%、34%。在540℃固溶处理时
含Ni的Mg
98-x
Er
2
Ni
x
合金组织结构未发生明显改变
仍为α-Mg相和LPSO相
且第二相未发生明显溶解
面积分数相比铸态合金有所增加。Mg
97.75
Er
2
Ni
0.25
、Mg
97.5
Er
2
Ni
0.5
和Mg
97
Er
2
Ni
1
三种合金固溶处理20h后的LPSO相面积分数分别为16%、34%、42%。
Abstract
The effects of Ni content on the microstructure of Mg
98-x
Er
2
Ni
x
(x=0
0.25
0.5
1
mole fraction)alloy were investigated by means of OM(optical microscope)
XRD(X-ray diffraction)
SEM(scanning electron microscope)and EDS(energy dispersed spectrometer).The results show that the ascast Mg
98
Er
2
alloy is composed of primary dendriteα-Mg phase with segregation of components.The composition phases of the three alloys of Mg
97.5
Er
2
Ni
0.25
Mg
97.5
Er
2
Ni
0.5
and Mg
97
Er
2
Ni
1
are mainly composed ofα-Mg phase and LPSO phase.The area fraction of the second phase reach 12%
19%and34%
respectively.During solid solution treatment at 540℃
the structure change of Mg
98-x
Er
2
Ni
x
alloy can be ignored
and the second phase is not dissolved obviously.Compared with that of the as-cast alloys