Zhu heguo, Wu xu, Chen shi. Study on the composites fabricated by the method of microwave exothermic dispersion synthesis in Al-ZrO2-B reaction system[J]. Special Casting & Nonferrous Alloys, 2008,(S1):351-353.
Zhu heguo, Wu xu, Chen shi. Study on the composites fabricated by the method of microwave exothermic dispersion synthesis in Al-ZrO2-B reaction system[J]. Special Casting & Nonferrous Alloys, 2008,(S1):351-353.DOI:
微波热爆合成Al-ZrO2-B系铝基复合材料研究
摘要
采用微波加热方式反应合成了Al-ZrO2-B系铝基复合材料
探讨了反应过程的基本原理。试验表明
合成反应过程仅需3
6
min
且环境友好;未加B粉时
Al-ZrO2系的反应产物由α-Al2O3和Al3Zr组成
其中α-Al2O3为细小颗粒
Al3Zr为块状物
两者均匀分布于Al基体中;当加入B粉后
反应产物中的Al3Zr减少
同时新增了ZrB2增强体颗粒;在x(B)/x(ZrO2)为2时
Al3Zr基本消失
ZrB2也为细小颗粒
与α-Al2O3一同弥散分布于Al基体中
从而形成α-Al2O3和ZrB2复合增强的内生型Al基复合材料。
Abstract
The composites (α-Al2O3+ ZrB2)/Al fabricated by microwave exothermic dispersion (MXD) method in Al-ZrO2-B system were investigated. The MXD synthesis process has lasted for about 6 min and which is harmonious with environment When the x(B)/x(ZrO2) is zero
the reinforcements of the composites are composed of α-Al2O3 and Al3Zr
which are of fine grains and blocks respectively. When the x(B)/x(ZrO2) increases
the amount of Al3Zr phase decreases. When the x(B)/x(ZrO2) reaches 2
the Al3Zr phase almost eliminates and the reinforcements of the composite are made up of α-Al2O3 and ZrB2 which are good distribution in the aluminum matrix.