考察了定向凝固速率在0.5100μm/s范围内的Cu-55Sn亚包晶合金凝固组织及凝固速率对微观组织形态、界面温度及相含量的影响。结果表明,定向凝固组织由初生ε相、包晶η相和共晶体(η+Sn)组成。定向凝固速率在0.51·0μm/s范围内时,初生相连为一体,包晶相呈块状嵌于初生相内;当凝固速度大于5μm/s,组织为常见的包晶η相包裹ε相的板条状,其中ε相为领先相,不能形成ε相和η相等温界面的耦合生长,与最高界面生长温度假设的分析相一致。定向凝固过程中包晶转变不明显,包晶η相大部分由液相直接凝固而成,并且随冷却速度增大,凝固时间减少,包晶相含量先增后减,在10μm/s附近出现极值。
Effects of solidification structure and solidified rate on structural morphology, interfacial temperature and phase constituent of Cu-55Sn hypo-peritectic alloy have been investigated with directional solidification rate in the range of 0. 5-100μm. The results show that directional solidified phase constituent is composed of primary ε phase, peritectic rj phase and eutectic (η+Sn) phase. Bulky peritectic rj phase is embedded in primary e phase in the directional solidification Cu-55Sn hypo-eutectic alloy with directionally solidified rate in the range of 0. 5μm/s while with solidified rate more than 5 μm, the solidification structure remains the conventional plate structure, where peritectic rj phase coats primary e phase. Coupled growth in isothermal interface for peritectic rj phase and primary εphase can not be formed because primary e phase is prior phase, which is in accordance with analysis of top-interface temperature growth theory. Major peritectic η phase is directionally formed from the liquid phase during direction solidification process. In addition, with increasing in cooling rate and decreasing in solidification time, peritectic rj phase content is firstly increased then decreased, and the peak content of the peritectic rj phase can be observed with the directional solidification rate of about 10 μm.
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