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Densification Process and Mechanical Properties of Fe-Cu Powder Alloy Prepared by Different Pressing Force
- Vol. 39, Issue 5, Pages: 472-476(2019)
Published: 2019
DOI: 10.15980/j.tzzz.2019.05.003
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Published: 2019 ,
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[1]刘博,罗海玉,包转丽,马虎林.不同压制力制备Fe-Cu粉末合金的致密化与力学性能[J].特种铸造及有色合金,2019,39(05):472-476.
Liu Bo, Luo Haiyu, Bao Zhuanli, et al. Densification Process and Mechanical Properties of Fe-Cu Powder Alloy Prepared by Different Pressing Force. [J]. Special Casting & Nonferrous Alloys 39(5):472-476(2019)
基于Fe-Cu系粉末冶金产品性能要求
采用单向压制方法并在确定烧结温度前提下
使用不同压制参数(压制力、压制速度)制备Fe-0.2Cu合金;利用XRD、OM、SEM等表征手段分析材料的微观组织、致密化过程与力学性能。结果表明
随着压制力增加
颗粒间结合度提高
界面尺寸减小
孔隙率降低且球化程度提高
组织更加均匀;当压制力为600MPa、压制速度为5.0m/s时
密度为6.9g/cm
3
在1 140℃烧结体抗拉强度为605MPa
硬度(HV)为230;基体相Fe以单质形式存在
Fe和Cu扩散形成了Fe
4
Cu
3
、Cu
9.9
Fe
0.1
等相
分布在孔隙或界面处
部分被氧化为Fe
3
O
4
、FeO和CuO;拉伸断口形貌呈现韧窝、解理河流花纹混合特征
断口孔隙形状由粗大不规则形状向细小球形转变
断裂形式从脆性沿晶断裂转为脆-韧性混合断裂。
Based on the performance requirements of Fe-Cu powder metallurgy products
the Fe-0.2 Cu alloy was prepared by unidirectional pressing method with different pressing parameters including pressing force and pressing speed at the determined sintering temperature.And microstructure
densification process and mechanical properties of the Fe-0.2 Cu alloy were analyzed by means of XRD
OM
SEM.The results show that the binding degree and the spheroidization degree in particles are increased while the interface size and the porosity are decreased with the increase of pressure
and the more uniform structure in the alloy can be observed.The maximum density
tensile strength and microhardness value of the prepared alloy reach up to 6.9 g/cm
3
605 MPa at 1 140℃ and 230 HV
respectively
with the pressing pressure of 600 MPa and pressing speed of 5.0 m/s.Iron matrix exists widely in form of single element.Fe atoms and Cu atoms are diffused to form phase such as Fe
4
Cu
3
Cu
9.9
Fe
0.1
which are located at cracks or surface and some of which oxidized to generate Fe
3
O
4
、FeO and CuO.The tensile fracture morphology shows that the pore shape of fracture is changed from coarse and irregular to small and regular sphere
which present the mixed characteristics of dimple
cleavage surface
tearing ridge and cleavage fluvial pattern.The fracture mode is changed from brittle fracture features to brittle-ductile with the increased force.
Fe-Cu合金压制力断裂方式
Fe-Cu AlloyPressing ForceFracture Mode
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