Yin Lu1, Wang Ge2, Zhang Linlin1, et al. Bonding Strength of TiN Plated Pure Ti and Solidex. [J]. Special Casting & Nonferrous Alloys (1):18-20(2008)DOI:
Bonding Strength of TiN Plated Pure Ti and Solidex
摘要
在纯Ti表面磁控溅射镀制不同Si含量的TiSiN膜后
比较与Solidex的结合强度并对界面进行分析。试验采用3组纯Ti试件
一组表面不作处理
另两组应用磁控溅射设备镀制不同Si含量的TiSiN膜后烤塑
采用AGS万能材料试验机测试纯Ti与Solidex的结合强度
并应用电子探针显微分析仪观察分析镀膜层-树脂界面。经方差分析显示
镀膜组结合强度优于未镀膜组
镀膜组中提高Si含量增加了结合强度
镀膜组中形成致密非晶态TiN、SiNx
它填补了金属基底与Solidex烤塑专用树脂可能存在的空隙
有助于阻止金属离子渗出。
Abstract
The bonding strength and interface morphology of pure Ti that is plated TiSiN film with different Si content by the magnetron sputtering method and Solidex were investigated by AGS materials testing machine and EMPA(electron microscope probe analysis).Variance analysis reveals that the bonding strength of TiSiN plated pure Ti and Solidex is superior to that of the pure Ti and the Solidex
furthermore
the bonding strength can be increased with increasing in Si content in TiSiN film.The compact amorphous TiN and SiNx phase can be generated in the film and be filled into the porosity between the metal matrix and Solidex light-cured hard crown and bridge composites
which is helpful for preventing the leakage of metal ion from the film
so the bonding strength is improved.
关键词
纯Ti磁控溅射镀膜TiSiN光固化冠桥树脂结合强度
Keywords
Pure TiMagnetron SputteringFilm-platedTiNLight-cured Hard Crown and Bridges CompositesBonding Strength