Li Guirong, Chen Ruilong, Zhao Yutao, et al. Apparent Viscosity of In-situ Synthesized Particulate Reinforced Aluminum Matrix Composites. [J]. Special Casting & Nonferrous Alloys (7):496-498(2008)DOI:
Apparent Viscosity of In-situ Synthesized Particulate Reinforced Aluminum Matrix Composites
摘要
选用Al-Zr(CO3)2反应组元
通过熔体直接反应法原位合成了(Al3Zr+Al2O3)p/Al颗粒增强铝基复合材料
增强颗粒粒度为0.5
3
.0μm。采用旋转柱体法测试了合成过程中复合材料熔体的表观粘度。结果表明
颗粒体积分数为5%时
熔体表观粘度-时间曲线呈抛物线形状
25min后粘度稳定在0.75Pa.s
较纯铝的0.24Pa.s增加了两倍多
原因是悬浮于铝液中的增强颗粒属于微米级
凝固组织中颗粒分布弥散均匀;颗粒体积分数为15%时
熔体表观粘度随时间增加逐渐上升
凝固组织中出现颗粒团聚现象。因此在原位合成复合材料工艺中
要综合考虑反应物加入量与收得率之间的关系
以及熔体表观粘度与凝固组织的关系。
Abstract
In-situ (Al3Zr+Al2O3)/Al particulate reinforced aluminum matrix composites was synthesized by direct melt reaction method in Al-Zr(CO3) system with the reinforced particulate size of 0.5
3
μm. The apparent viscosity of the composites melt during synthesized process was measured with rotary cylinder method. The results indicate that apparent viscosity via time curves of the composites with 5% particle volumetric fraction belongs to a parabolic one
and keeps a constant value of 0.75 Pas after 25 min and is two times higher than that of 0.24 Pas of pure aluminum
which is attributed to the uniform and dispersive distribution of micron particulate in composites. Melt apparent viscosity of the composites with 15% particulate volumetric fraction is increased with the increase of time
and the particulate aggregation can be observed in the microstructure.