Wang Ping, Li Jianping, Ma Qun. Optimization of Electrolyte Formula of Micro-arc Oxidation for Mg-9Gd-3Y-0.6Zn-0.5Zr Magnesium Alloy in Aluminate Solution. [J]. Special Casting & Nonferrous Alloys (7):502-504(2008)
Wang Ping, Li Jianping, Ma Qun. Optimization of Electrolyte Formula of Micro-arc Oxidation for Mg-9Gd-3Y-0.6Zn-0.5Zr Magnesium Alloy in Aluminate Solution. [J]. Special Casting & Nonferrous Alloys (7):502-504(2008)DOI:
Optimization of Electrolyte Formula of Micro-arc Oxidation for Mg-9Gd-3Y-0.6Zn-0.5Zr Magnesium Alloy in Aluminate Solution
摘要
采用铝酸盐体系对Mg-9Gd-3Y-0.6Zn-0.5Zr镁合金进行了微弧氧化处理
并通过扫描电镜、X射线衍射、电化学测试技术等方法
研究了不同电解液浓度下微弧氧化膜层耐蚀性能及其形貌特征。结果表明
经微弧氧化处理
合金的耐蚀性能明显提高。通过4因素3水平的正交试验
确定了铝酸盐体系中进行微弧氧化处理电解液的最优配方:NaAlO2的质量浓度为5g/L
H2O2的体积浓度为1.0%
KF的质量浓度为6g/L
丙三醇的体积浓度为1.5%。所得膜层厚度均匀
主要由MgO、Al2O3和MgAl2O4组成
含有少量的MgF2存在。
Abstract
The Mg-9Gd-3Y-0.6Zn-0.5Zr magnesium alloy was treated by micro-arc oxidation in aluminite solution
and morphology and corrosion resistance of oxide coating at different electrolyte were investigated by SEM (scanning electron microscope)
X-ray and electrochemical testing. The results indicate that the corrosion resistance of the alloy can be greatly improved by MAO treatment. The optimized processing parameters as follows: NaAlO2 of 5 g/L
H2O2 of 10mL/L
KF of 6g/L
glycerine of 15 mL/L. The coating with uniform thickness consists of MgO
State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology,Lanzhou 7300502. Key Laboratory of Non-ferrous Metal Alloys and Processing, The Ministry of Education,Lanzhou University of Technology
兰州理工大学有色金属合金及加工教育部重点实验室
State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials,Lanzhou University ofTechnology
School of Mechanical and Power Engineering, Shenyang University of Chemical Technology
School of Mechanical Engineering, Northwestern Polytechnical University