Zhu Hao, Zhao Zhongmin, Zhang Long, et al. Composition,Microstructure and Properties of Al2O3/ZrO2(4Y)Composites Prepared by Combustion Synthesis under High Gravity. [J]. Special Casting & Nonferrous Alloys 29(5):455-458(2009)
Zhu Hao, Zhao Zhongmin, Zhang Long, et al. Composition,Microstructure and Properties of Al2O3/ZrO2(4Y)Composites Prepared by Combustion Synthesis under High Gravity. [J]. Special Casting & Nonferrous Alloys 29(5):455-458(2009)DOI:
Composition,Microstructure and Properties of Al2O3/ZrO2(4Y)Composites Prepared by Combustion Synthesis under High Gravity
/ZrO2(4Y)composite ceramics with various component and structure were prepared by combustion synthesis under high gravity
and the correlation of component
microstructure and mechanical properties of composite ceramics were investigated by XRD(X-ray diffraction)
SEM(scanning electron microscope)and EDS(energy dispersive spectrum).The results reveal that Al
2
O
3
/33ZrO2(4Y)is composed of random-oriented rode-shape colonies embedding by a triangular dispersion of orderly t-ZrO2 submicron fibers
surrounded by inter-colony regions consisting of nano-micrometer spherically-shape t-ZrO2 grains
meanwhile
Al
2
O
3
/40ZrO2(4Y)is composed of micronmeter spherically-shape t-ZrO2
surrounded by irregular-shape α-Al
2
O
3
grains and a few colonies.Compared with the international directionally-solidified Al
2
O
3
/ZrO2(Y2O3)
the increase of hardness and flexural strength of Al
2
O
3
/33ZrO2(4Y)are attributed to high densification
small-size defects and high fracture toughness induced by compressive residual stress toughening and transformation toughening mechanism.In addition
in despite of the moderate decrease in hardness
flexural strength and fracture toughness are increased by 19.0% and 311.1%
respectively
which is attributed to the result of small-size defect in micron-meter spherically-shaped t-ZrO2 grain matrix and high fracture toughness induced by stress-induced t-ZrO2 transformation toughening and transformation-induced micro-crack toughening mechanisms.
关键词
Al2O3/ZrO2(4Y)燃烧合成超重力自生长强韧化
Keywords
Al2O3/ZrO2(4Y)Combustion SynthesisHigh GravitySelf-growthReinforcing and Toughening