Xu Jinghua1, Geng Haoran1, Sun Jiawei2, et al. Preparation and Performance of the Fe3Al Intermetallic Network Structure Materials. [J]. Special Casting & Nonferrous Alloys 30(4):364-366(2010)
Xu Jinghua1, Geng Haoran1, Sun Jiawei2, et al. Preparation and Performance of the Fe3Al Intermetallic Network Structure Materials. [J]. Special Casting & Nonferrous Alloys 30(4):364-366(2010)DOI:
Preparation and Performance of the Fe3Al Intermetallic Network Structure Materials
摘要
采用机械合金化法、退火工艺和热处理工艺制备了Fe3Al网络结构多孔材料
通过扫描电镜、XRD观察分析了该结构材料的形貌特征
研究了烧结温度、升温速度、孔隙率对该材料的抗压强度和断裂韧度的影响
并初步探讨了材料的断裂机理。结果表明
随着烧结温度的升高
Fe3Al多孔材料中的孔筋逐渐致密
1420℃烧结时
材料的组织、性能最好
烧结温度继续升高时材料出现明显坍塌变形
不利于材料的成形。孔隙率是影响Fe3Al多孔材料力学性能的主要因素
通过较低的烧结升温速率可降低孔隙率
获得结构致密的骨架
从而有助于提高多孔材料的抗压强度和断裂韧度。利用桥接和自愈合机理探讨了改善多孔材料力学性能的途径
通过添加Ti和控制适量的孔洞
提高了材料的抗压强度和断裂韧度。
Abstract
Fe3Al intermetallic network structural materials were prepared by mechanical alloying
annealing and heat treatment
and effects of sintering temperature
temperature increment rate
porosity on compressive strength and fracture toughness of the materials were investigated through observing morphology using SEM (scanning electron microscope)
XRD (X-ray diffraction)
meanwhile
fracture mechanism of the materials were approached also. The results demonstrate that with increasing in sintering temperature
porosity in the Fe3Al intermetallics is gradually densified
and desirable structure and performance can be obtained with sintering at 1420℃
however
it is deteriorated for formation of the materials as a result of evidently collapsed deformation with further increasing in sintering temperature. Mechanical properties of the Fe3Al materials are mainly controlled by porosity rate. Porosity rate can be decreased with a lower sintering temperature-increment rate
which is beneficial for improving compressive strength and fracture toughness of the materials due to generation of frame with compact structure. Based on bridge theory and self-healing mechanism
ways of improving mechanical properties of the materials were described. Through adding Ti element and controlling proper porosity rate
compressive strength and fracture toughness of the materials were improved.